Information card for entry 4077343

Structure parameters

• Formula: C35 H23 Cl2 N O5 Ru2
• Calculated formula: C34 H21 Cl N O5 Ru2
• Title of publication: Reactivity of [Ru2(μ-η1:η1-NCPh2)(μ-η1:η2-PhCCHPh)(CO)6] with Alkynes. Insertion Reactions of Nonactivated Alkynes into Ru−C and Ru−N Bonds
• Authors of publication: Cabeza, Javier A.; del Río, Ignacio; Grepioni, Fabrizia; Moreno, Marta; Riera, Víctor; Suárez, Marta
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 20
• Pages of publication: 4190
• a: 9.32 ± 0.008 Å
• b: 17.77 ± 0.009 Å
• c: 16.396 ± 0.003 Å
• α: 90°
• β: 95.34 ± 0.04°
• γ: 90°
• Cell volume: 2704 ± 3 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1244
• Residual factor for significantly intense reflections: 0.06
• Weighted residual factors for significantly intense reflections: 0.1584
• Weighted residual factors for all reflections included in the refinement: 0.1931
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No