Information card for entry 4077387

Structure parameters

• Formula: C42 H68 N2 Os2 P2 Pt S2 Si4
• Calculated formula: C42 H68 N2 Os2 P2 Pt S2 Si4
• SMILES: [Os]1([S]2[Os]([S]1[Pt]12[P](CC[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)(#N)(C[Si](C)(C)C)C[Si](C)(C)C)(#N)(C[Si](C)(C)C)C[Si](C)(C)C
• Title of publication: Synthesis of (dppe)Pt(μ3-S)2{Ru(N)Me2}2, (dppe)Pt(μ3-S)2{Os(N)(CH2SiMe3)2}2, and Related Heterometallic Complexes
• Authors of publication: Shapley, Patricia A.; Liang, Hong-Chang; Dopke, Nancy C.
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 22
• Pages of publication: 4700
• a: 11.8022 ± 0.0004 Å
• b: 21.4284 ± 0.0008 Å
• c: 21.2654 ± 0.0007 Å
• α: 90°
• β: 99.166 ± 0.001°
• γ: 90°
• Cell volume: 5309.4 ± 0.3 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.089
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0521
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 0.834
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No