Information card for entry 4077404

Structure parameters

• Formula: C24 H36 B10 O2 Si
• Calculated formula: C24 H36 B10 O2 Si
• SMILES: [Si]1(OC([C]2345[BH]678[BH]9%10%11[BH]%12%13%14[BH]%1569[BH]637[BH]3%14%15[BH]79%13[BH]%13%10%12[BH]27([BH]48%11%13)[C]5639C(O1)/C=C/c1ccccc1)/C=C/c1ccccc1)(CC)CC
• Title of publication: Palladium-Catalyzed Double-Silylation Reactions of 3,4-Carboranylene-1,1,2,2-tetraethyl-1,2-disilacyclobut-3-ene
• Authors of publication: Song, Kyu Ho; Jung, Il; Lee, Shim Sung; Park, Ki-Min; Ishikawa, Mitsuo; Kang, Sang Ook; Ko, Jaejung
• Journal of publication: Organometallics
• Year of publication: 2001
• Journal volume: 20
• Journal issue: 26
• Pages of publication: 5537
• a: 10.6814 ± 0.0009 Å
• b: 11.6686 ± 0.0011 Å
• c: 12.4992 ± 0.0012 Å
• α: 75.755 ± 0.002°
• β: 74.57 ± 0.002°
• γ: 73.167 ± 0.002°
• Cell volume: 1413 ± 0.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1029
• Residual factor for significantly intense reflections: 0.0542
• Weighted residual factors for significantly intense reflections: 0.1338
• Weighted residual factors for all reflections included in the refinement: 0.1571
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No