Crystallography Open Database

Information card for entry 4077431

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Coordinates	4077431.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C55 H51 Cl2 P3 Ru Si
Calculated formula	C55 H50.01 Cl2 P3 Ru Si
Title of publication	RuH3(SiCl2Me)(PPh3)3: A Trihydridosilylruthenium Complex with Three Nonclassical Ru−H···Si Interactions
Authors of publication	Yardy, Nicholas M.; Lemke, Frederick R.; Brammer, Lee
Journal of publication	Organometallics
Year of publication	2001
Journal volume	20
Journal issue	26
Pages of publication	5670
a	23.7603 ± 0.0004 Å
b	14.6024 ± 0.0003 Å
c	13.9643 ± 0.0003 Å
α	90°
β	90°
γ	90°
Cell volume	4845.02 ± 0.17 Å³
Cell temperature	183 ± 2 K
Ambient diffraction temperature	183 ± 2 K
Number of distinct elements	6
Space group number	33
Hermann-Mauguin space group symbol	P n a 21
Hall space group symbol	P 2c -2n
Residual factor for all reflections	0.0272
Residual factor for significantly intense reflections	0.0239
Weighted residual factors for significantly intense reflections	0.0634
Weighted residual factors for all reflections included in the refinement	0.0652
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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