Information card for entry 4077529

Structure parameters

• Formula: C10 H21 F3 O6 Os P2 S
• Calculated formula: C10 H21 F3 O6 Os P2 S
• Title of publication: Cationic Osmium(II) Acetyl Complexes Bearing Pyrazolylmethane Ligands: Intramolecular and Interionic Structure and Isolation of an Intermediate Containing the “Os−I−Ag” Moiety
• Authors of publication: Bellachioma, Gianfranco; Cardaci, Giuseppe; Macchioni, Alceo; Valentini, Francesco; Zuccaccia, Cristiano; Foresti, Elisabetta; Sabatino, Piera
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 21
• Pages of publication: 4320
• a: 8.742 Å
• b: 23.683 Å
• c: 10.049 Å
• α: 90°
• β: 106.87°
• γ: 90°
• Cell volume: 1990.98 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0659
• Residual factor for significantly intense reflections: 0.0405
• Weighted residual factors for significantly intense reflections: 0.1003
• Weighted residual factors for all reflections included in the refinement: 0.1069
• Goodness-of-fit parameter for all reflections included in the refinement: 1.354
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No