Information card for entry 4077719

Structure parameters

• Chemical name: catena-Poly{[tetrakis(μ-trifluoroacetato-κO,kO')dirhodium(II,II)]- -η2,-η2-diphenylacetylene}
• Formula: C22 H10 F12 O8 Rh2
• Calculated formula: C22 H10 F12 O8 Rh2
• Title of publication: Studies of Dirhodium(II) Tetrakis(trifluoroacetate). 6. The First Structural Characterization of Axial Alkyne Complexes, Rh2(O2CCF3)4(Ph2C2)n(n= 1, 2): Diphenylacetylene as a Bifunctional Ligand
• Authors of publication: Cotton, F. Albert; Dikarev, Evgeny V.; Petrukhina, Marina A.; Stiriba, Salah-Eddine
• Journal of publication: Organometallics
• Year of publication: 2000
• Journal volume: 19
• Journal issue: 7
• Pages of publication: 1402
• a: 9.303 ± 0.0004 Å
• b: 9.5423 ± 0.0009 Å
• c: 16.3049 ± 0.0006 Å
• α: 76.795 ± 0.004°
• β: 84.24 ± 0.005°
• γ: 68.653 ± 0.004°
• Cell volume: 1312.23 ± 0.15 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0411
• Residual factor for significantly intense reflections: 0.0378
• Weighted residual factors for all reflections: 0.0972
• Weighted residual factors for significantly intense reflections: 0.0935
• Goodness-of-fit parameter for all reflections: 1.043
• Goodness-of-fit parameter for significantly intense reflections: 1.049
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No