Information card for entry 4077729

Structure parameters

• Formula: C34 H37 F15 N2 Pd
• Calculated formula: C34 H37 F15 N2 Pd
• Title of publication: Reactivity of [{M(C6F5)2(μ-OH)}2]2-(M = Pd or Pt) toward Aromatic Amines and Malononitrile
• Authors of publication: Ruiz, José; Rodríguez, Venancio; López, Gregorio; Casabó, Jaume; Molins, Elies; Miravitlles, Carles
• Journal of publication: Organometallics
• Year of publication: 1999
• Journal volume: 18
• Journal issue: 7
• Pages of publication: 1177
• a: 12.567 ± 0.003 Å
• b: 17.637 ± 0.006 Å
• c: 17.016 ± 0.004 Å
• α: 90 ± 0.02°
• β: 97.88 ± 0.02°
• γ: 90 ± 0.02°
• Cell volume: 3735.9 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1934
• Residual factor for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections: 0.2425
• Weighted residual factors for significantly intense reflections: 0.1751
• Goodness-of-fit parameter for all reflections: 1.048
• Goodness-of-fit parameter for significantly intense reflections: 1.234
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No