Crystallography Open Database

Information card for entry 4077972

Preview

Coordinates	4077972.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22.44 H32.88 Cl2.88 N2 O2 Pt
Calculated formula	C22 H32 Cl2 N2 O2 Pt
Title of publication	Gyroscope-Like Platinum and Palladium Complexes with Trans-Spanning Bis(pyridine) Ligands
Authors of publication	Zeits, Paul D.; Rachiero, Giovanni Pietro; Hampel, Frank; Reibenspies, Joseph H.; Gladysz, John A.
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	7
Pages of publication	2854
a	12.6145 ± 0.0002 Å
b	12.6662 ± 0.0003 Å
c	18.3536 ± 0.0005 Å
α	102.97 ± 0.001°
β	101.277 ± 0.001°
γ	112.874 ± 0.001°
Cell volume	2498.95 ± 0.1 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.049
Weighted residual factors for significantly intense reflections	0.1421
Weighted residual factors for all reflections included in the refinement	0.1526
Goodness-of-fit parameter for all reflections included in the refinement	1.061
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4077972.html