Information card for entry 4078034

Structure parameters

• Formula: C32 H30 Cu F6 N7 O P2
• Calculated formula: C32 H30 Cu F6 N7 O P2
• Title of publication: Tris(pyrazolyl)phosphine Oxides. Synthesis and Coordination Chemistry with Copper(I)
• Authors of publication: Tazelaar, Cornelis G. J.; Lyaskovskyy, Volodymyr; Dijk, Tom van; Broere, Daniël L. J.; Kolfschoten, Ludo A.; Khiar, Rima Osman Hassan; Lutz, Martin; Slootweg, J. Chris; Lammertsma, Koop
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 8
• Pages of publication: 3308
• a: 8.612 ± 0.0003 Å
• b: 23.4829 ± 0.0009 Å
• c: 17.3556 ± 0.0006 Å
• α: 90°
• β: 109.357 ± 0.002°
• γ: 90°
• Cell volume: 3311.5 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0337
• Residual factor for significantly intense reflections: 0.0294
• Weighted residual factors for significantly intense reflections: 0.0761
• Weighted residual factors for all reflections included in the refinement: 0.0795
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No