Information card for entry 4078188

Structure parameters

• Formula: C25 H39 Cl2 N3 P Rh
• Calculated formula: C25 H39 Cl2 N3 P Rh
• Title of publication: N–H Activation by Rh(I) via Metal–Ligand Cooperation
• Authors of publication: Feller, Moran; Diskin-Posner, Yael; Shimon, Linda J. W.; Ben-Ari, Eyal; Milstein, David
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 11
• Pages of publication: 4083 - 4101
• a: 14.1476 ± 0.0005 Å
• b: 24.9498 ± 0.0009 Å
• c: 7.5796 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2675.45 ± 0.17 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0429
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0858
• Weighted residual factors for all reflections included in the refinement: 0.0881
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No