Information card for entry 4078281

Structure parameters

• Formula: C47.66 H51.96 Cl0.34 F6 N5 O6.88 Pd S2
• Calculated formula: C47.652 H51.956 Cl0.348 F6 N5 O6.884 Pd S2
• Title of publication: Synthesis of Palladium(II), -(III), and -(IV) Complexes with Acyclic Diaminocarbene Ligands
• Authors of publication: Mart\?ínez-Mart\?ínez, Antonio-Jesús; Chicote, María-Teresa; Bautista, Delia; Vicente, José
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 9
• Pages of publication: 3711
• a: 10.2499 ± 0.0005 Å
• b: 14.6931 ± 0.0007 Å
• c: 17.9342 ± 0.0009 Å
• α: 71.603 ± 0.002°
• β: 78.117 ± 0.002°
• γ: 74.951 ± 0.002°
• Cell volume: 2452.3 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0427
• Residual factor for significantly intense reflections: 0.0374
• Weighted residual factors for significantly intense reflections: 0.0856
• Weighted residual factors for all reflections included in the refinement: 0.0881
• Goodness-of-fit parameter for all reflections included in the refinement: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No