Crystallography Open Database

Information card for entry 4078354

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Coordinates	4078354.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23.5 H34 Cl2 Sn2
Calculated formula	C23.5 H30 Cl2 Sn2
Title of publication	Synthesis and Characterization of Sn(η5-C5Me5)Cl and Sn{η5-C5Me4(SiMe2But)}Cl
Authors of publication	Constantine, Steven P.; De Lima, Geraldo M.; Hitchcock, Peter B.; Keates, Julian M.; Lawless, Gerard A.; Marziano, Ivan
Journal of publication	Organometallics
Year of publication	1997
Journal volume	16
Journal issue	4
Pages of publication	793
a	10.029 ± 0.003 Å
b	11.577 ± 0.005 Å
c	11.838 ± 0.004 Å
α	77.34°
β	75.98 ± 0.03°
γ	75.61°
Cell volume	1273.1 ± 0.8 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0357
Residual factor for significantly intense reflections	0.0285
Weighted residual factors for all reflections	0.0722
Weighted residual factors for significantly intense reflections	0.0679
Goodness-of-fit parameter for all reflections	0.967
Goodness-of-fit parameter for significantly intense reflections	0.981
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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