Information card for entry 4078415

Structure parameters

• Common name: compound 9
• Formula: C44 H48 Li2 P2
• Calculated formula: C44 H48 Li2 P2
• Title of publication: New Lithium Phosphonium Diylides: A Methylene and a Cyclopentadienyl Moiety as Ylidic Coordination Sites
• Authors of publication: Lichtenberg, Crispin; Hillesheim, Nina S.; Elfferding, Michael; Oelkers, Benjamin; Sundermeyer, Jörg
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 11
• Pages of publication: 4259
• a: 8.5472 ± 0.0004 Å
• b: 11.2691 ± 0.0006 Å
• c: 19.6735 ± 0.0009 Å
• α: 91.412 ± 0.004°
• β: 90.728 ± 0.004°
• γ: 100.064 ± 0.004°
• Cell volume: 1864.93 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0516
• Residual factor for significantly intense reflections: 0.0344
• Weighted residual factors for significantly intense reflections: 0.0822
• Weighted residual factors for all reflections included in the refinement: 0.0859
• Goodness-of-fit parameter for all reflections included in the refinement: 0.895
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No