An Oligosilsesquioxane Cage Functionalized with Molybdenum(II) Organometallic Fragments
Authors of publication
Dias Filho, Newton L.; Portugal, Fátima C. M.; Nogueira, J. M. F.; Brandão, Paula; Félix, Vitor; Vaz, Pedro D.; Nunes, Carla D.; Veiros, Luis F.; Brito, Maria J. Villa de; Calhorda, Maria José
Journal of publication
Organometallics
Year of publication
2012
Journal volume
31
Journal issue
12
Pages of publication
4495
a
10.2067 ± 0.0006 Å
b
15.2037 ± 0.0009 Å
c
15.5094 ± 0.0009 Å
α
99.157 ± 0.003°
β
103.552 ± 0.003°
γ
99.353 ± 0.003°
Cell volume
2259.3 ± 0.2 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0928
Residual factor for significantly intense reflections
0.0585
Weighted residual factors for significantly intense reflections
0.1606
Weighted residual factors for all reflections included in the refinement
0.1908
Goodness-of-fit parameter for all reflections included in the refinement
