Information card for entry 4078902

Structure parameters

• Formula: C14 H20 I3 N5 O2 Rh
• Calculated formula: C14 H21 I3 N5 O2 Rh
• Title of publication: Rhodium and Iridium Complexes with ChelatingC‒C′-Imidazolylidene‒Pyridylidene Ligands: Systematic Approach to Normal, Abnormal, and Remote Coordination Modes
• Authors of publication: Segarra, Candela; Mas-Marzá, Elena; Mata, José A.; Peris, Eduardo
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 14
• Pages of publication: 5169
• a: 7.3202 ± 0.0006 Å
• b: 11.6155 ± 0.0013 Å
• c: 27.281 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2319.6 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.063
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0931
• Goodness-of-fit parameter for all reflections included in the refinement: 1.212
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MOKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No