Synthesis, Structure, Dynamics, and Selective Methylation of Platinum and Palladium Diphosphametallacyclobutane Complexes
Authors of publication
Chapp, Timothy W.; Schoenfeld, Adam J.; Sanderson, Matthew D.; Chang, Cory L.; Glueck, David S.; Golen, James A.; Moore, Curtis E.; Rheingold, Arnold L.
Journal of publication
Organometallics
Year of publication
2012
Journal volume
31
Journal issue
15
Pages of publication
5573
a
33.225 ± 0.009 Å
b
9.898 ± 0.003 Å
c
18.448 ± 0.004 Å
α
90°
β
121.377 ± 0.003°
γ
90°
Cell volume
5180 ± 2 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0505
Residual factor for significantly intense reflections
0.0396
Weighted residual factors for significantly intense reflections
0.1189
Weighted residual factors for all reflections included in the refinement
0.1263
Goodness-of-fit parameter for all reflections included in the refinement
