Information card for entry 4078938

Structure parameters

• Formula: C46 H65 Cl Y2
• Calculated formula: C46 H64.98 Cl Y2
• Title of publication: Reactivity of the Y3+Tuck-Over Hydride Complex, (C5Me5)2Y(μ-H)(μ-CH2C5Me4)Y(C5Me5)
• Authors of publication: Schmiege, Benjamin M.; Fieser, Megan E.; Ziller, Joseph W.; Evans, William J.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 15
• Pages of publication: 5591
• a: 19.2433 ± 0.0006 Å
• b: 16.9361 ± 0.0006 Å
• c: 14.1667 ± 0.0005 Å
• α: 90°
• β: 116.072 ± 0.0004°
• γ: 90°
• Cell volume: 4147.2 ± 0.2 ų
• Cell temperature: 98 ± 2 K
• Ambient diffraction temperature: 98 ± 2 K
• Number of distinct elements: 4
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0285
• Residual factor for significantly intense reflections: 0.0253
• Weighted residual factors for significantly intense reflections: 0.0608
• Weighted residual factors for all reflections included in the refinement: 0.062
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No