Information card for entry 4078947

Structure parameters

• Formula: C37 H86 Li4 N7 Si4
• Calculated formula: C37 H86 Li4 N7 Si4
• Title of publication: The [(DABCO)7·(LiCH2SiMe3)8] Octamer: More Aggregated than the Parent Starting Material [LiCH2SiMe3]6but Also Higher in Reactivity
• Authors of publication: Tatić, Tanja; Hermann, Stefanie; Stalke, Dietmar
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 15
• Pages of publication: 5615
• a: 9.5014 ± 0.0006 Å
• b: 16.8738 ± 0.001 Å
• c: 17.3714 ± 0.001 Å
• α: 64.013 ± 0.001°
• β: 88.208 ± 0.001°
• γ: 78.191 ± 0.001°
• Cell volume: 2445.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0483
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0899
• Weighted residual factors for all reflections included in the refinement: 0.0965
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No