Crystallography Open Database

Information card for entry 4079106

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Coordinates	4079106.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C66 H93 N O2 Sn
Calculated formula	C66 H93 N O2 Sn
Title of publication	Versatile Reactivity of Stannene Tip2Sn═CR2with Unsaturated Compounds
Authors of publication	Fatah, Abdoul; Ghereg, Dumitru; Escudié, Jean; Saffon, Nathalie; Ladeira, Sonia; Ranaivonjatovo, Henri
Journal of publication	Organometallics
Year of publication	2012
Journal volume	31
Journal issue	17
Pages of publication	6148
a	13.6754 ± 0.0003 Å
b	14.4472 ± 0.0004 Å
c	16.8577 ± 0.0004 Å
α	90.391 ± 0.002°
β	107.263 ± 0.002°
γ	107.259 ± 0.002°
Cell volume	3020.87 ± 0.14 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1153
Residual factor for significantly intense reflections	0.0585
Weighted residual factors for significantly intense reflections	0.0973
Weighted residual factors for all reflections included in the refinement	0.116
Goodness-of-fit parameter for all reflections included in the refinement	0.977
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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