Information card for entry 4079605

Structure parameters

• Formula: C68 H82 N6 O2 Si2
• Calculated formula: C68 H82 N6 O2 Si2
• Title of publication: Reactivity Studies of Heteroleptic Silylenes with N2O
• Authors of publication: Azhakar, Ramachandran; Pröpper, Kevin; Dittrich, Birger; Roesky, Herbert W.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 21
• Pages of publication: 7586
• a: 12.4224 ± 0.0003 Å
• b: 11.5174 ± 0.0003 Å
• c: 21.055 ± 0.0006 Å
• α: 90°
• β: 101.291 ± 0.001°
• γ: 90°
• Cell volume: 2954.11 ± 0.13 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.036
• Weighted residual factors for significantly intense reflections: 0.1026
• Weighted residual factors for all reflections included in the refinement: 0.1195
• Goodness-of-fit parameter for all reflections included in the refinement: 1.163
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No