Information card for entry 4080118

Structure parameters

• Formula: C91.67 H139.67 N6 O4.17 Yb2
• Calculated formula: C91.6667 H139.667 N6 O4.16667 Yb2
• Title of publication: Reactivity of Ytterbium(II) Hydride. Redox Reactions: Ytterbium(II) vs Hydrido Ligand. Metathesis of the Yb‒H Bond
• Authors of publication: Basalov, Ivan V.; Lyubov, Dmitry M.; Fukin, Georgy K.; Cherkasov, Anton V.; Trifonov, Alexander A.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 5
• Pages of publication: 1507
• a: 20.671 ± 0.002 Å
• b: 26.709 ± 0.003 Å
• c: 29.791 ± 0.003 Å
• α: 111.023 ± 0.002°
• β: 106.486 ± 0.003°
• γ: 97.723 ± 0.003°
• Cell volume: 14200 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.3462
• Residual factor for significantly intense reflections: 0.1105
• Weighted residual factors for significantly intense reflections: 0.1754
• Weighted residual factors for all reflections included in the refinement: 0.2314
• Goodness-of-fit parameter for all reflections included in the refinement: 0.823
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No