Information card for entry 4080502

Structure parameters

• Formula: C66 H58 B2 F24 N P Ru
• Calculated formula: C66 H58 B2 F24 N P Ru
• Title of publication: Aminoborane σ Complexes: Significance of Hydride Co-ligands in Dynamic Processes and Dehydrogenative Borylene Formation
• Authors of publication: Addy, David A.; Bates, Joshua I.; Kelly, Michael J.; Riddlestone, Ian M.; Aldridge, Simon
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 6
• Pages of publication: 1583
• a: 12.8893 ± 0.0002 Å
• b: 13.6791 ± 0.0003 Å
• c: 18.9851 ± 0.0004 Å
• α: 91.1751 ± 0.0009°
• β: 90.1685 ± 0.001°
• γ: 90.5343 ± 0.0008°
• Cell volume: 3346.47 ± 0.11 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1126
• Residual factor for significantly intense reflections: 0.0702
• Weighted residual factors for all reflections: 0.1767
• Weighted residual factors for significantly intense reflections: 0.1313
• Weighted residual factors for all reflections included in the refinement: 0.1767
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9332
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No