Information card for entry 4080762

Structure parameters

• Chemical name: Phtalimide-[1,2-bis(diisopropylphosphanyl)ethane-P,P]-chloro-nickel(II)
• Formula: C22 H36 Cl N Ni O2 P2
• Calculated formula: C22 H36 Cl N Ni O2 P2
• Title of publication: Selective C═O Reduction in Phthalimide with Nickel(0) Compounds
• Authors of publication: Arévalo, Alma; Ovando-Segovia, Sebastián; Flores-Alamo, Marcos; Garc\?ía, Juventino J.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 10
• Pages of publication: 2939
• a: 31.6164 ± 0.001 Å
• b: 13.6477 ± 0.0005 Å
• c: 16.4738 ± 0.0006 Å
• α: 90°
• β: 92.856 ± 0.003°
• γ: 90°
• Cell volume: 7099.5 ± 0.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0749
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.1605
• Weighted residual factors for all reflections included in the refinement: 0.1755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No