Information card for entry 4080880

Structure parameters

• Chemical name: Li4[(N(SiMe3)CH2CH2)2O]2
• Formula: C20 H52 Li4 N4 O2 Si4
• Calculated formula: C20 H52 Li4 N4 O2 Si4
• SMILES: C1C[O]2CC[N]3([Si](C)(C)C)[Li]4[N]5(CC[O]64CC[N]([Si](C)(C)C)([Li]23)[Li]6[N]1([Si](C)(C)C)[Li]5)[Si](C)(C)C
• Title of publication: Synthesis and Reactivity of Titanium Hydrazido Complexes Supported by Diamido-Ether Ligands
• Authors of publication: Unruangsri, Junjuda; Morgan, Hannah; Schwarz, Andrew D.; Schofield, A. Daniel; Mountford, Philip
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 10
• Pages of publication: 3091
• a: 10.3235 ± 0.0002 Å
• b: 12.5522 ± 0.0003 Å
• c: 14.3656 ± 0.0004 Å
• α: 91.4334 ± 0.0009°
• β: 108.448 ± 0.001°
• γ: 110.347 ± 0.001°
• Cell volume: 1636.49 ± 0.07 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1209
• Residual factor for significantly intense reflections: 0.0673
• Weighted residual factors for all reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.0342
• Weighted residual factors for all reflections included in the refinement: 0.0312
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0539
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No