Information card for entry 4081340

Structure parameters

• Formula: C149 H114 Cl2 F24 N20 P4 Ru4
• Calculated formula: C149 H114 Cl2 F24 N20 P4 Ru4
• Title of publication: Rational Synthesis of Heteroleptic Tris(chelate) Ruthenium Complexes [RuII(2-Ph-2′-Py)(L∧L)(L′∧L′)]PF6by Selective Substitution of the Ligand Trans to the Ruthenated Phenyl Ring
• Authors of publication: Boff, Bastien; Ali, Moussa; Alexandrova, Larissa; Espinosa-Jalapa, Noel Ángel; Saavedra-Díaz, Rafael Omar; Le Lagadec, Ronan; Pfeffer, Michel
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 18
• Pages of publication: 5092
• a: 27.441 ± 0.002 Å
• b: 14.3073 ± 0.0011 Å
• c: 18.6044 ± 0.0014 Å
• α: 90°
• β: 96.621 ± 0.001°
• γ: 90°
• Cell volume: 7255.5 ± 0.9 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.11
• Residual factor for significantly intense reflections: 0.0568
• Weighted residual factors for significantly intense reflections: 0.1149
• Weighted residual factors for all reflections included in the refinement: 0.1304
• Goodness-of-fit parameter for all reflections included in the refinement: 0.919
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No