Information card for entry 4081994

Structure parameters

• Formula: C16 H32 Ni O2 P2
• Calculated formula: C16 H32 Ni O2 P2
• Title of publication: Nickel-Catalyzed Hydrosilylation of CO2in the Presence of Et3B for the Synthesis of Formic Acid and Related Formates
• Authors of publication: González-Sebastián, Lucero; Flores-Alamo, Marcos; Garc\?ía, Juventino J.
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 23
• Pages of publication: 7186
• a: 32.567 ± 0.005 Å
• b: 11.0531 ± 0.0008 Å
• c: 16.7505 ± 0.0013 Å
• α: 90°
• β: 100.957 ± 0.012°
• γ: 90°
• Cell volume: 5919.7 ± 1.1 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0795
• Residual factor for significantly intense reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.0974
• Weighted residual factors for all reflections included in the refinement: 0.1144
• Goodness-of-fit parameter for all reflections included in the refinement: 1.02
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No