Information card for entry 4082300

Structure parameters

• Formula: C59 H89 B Br N4 P3 Ru
• Calculated formula: C59 H89 B Br N4 P3 Ru
• Title of publication: Synthesis and Reactivity of Ruthenium Hydride Complexes Containing a Tripodal Aminophosphine Ligand
• Authors of publication: Sgro, Michael J.; Dahcheh, Fatme; Stephan, Douglas W.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 2
• Pages of publication: 578
• a: 12.4309 ± 0.0007 Å
• b: 14.0726 ± 0.001 Å
• c: 19.3979 ± 0.0013 Å
• α: 94.222 ± 0.004°
• β: 96.622 ± 0.004°
• γ: 114.566 ± 0.003°
• Cell volume: 3037.7 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1136
• Residual factor for significantly intense reflections: 0.0737
• Weighted residual factors for significantly intense reflections: 0.195
• Weighted residual factors for all reflections included in the refinement: 0.2128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No