Photochemistry of Chromium Arene Tricarbonyl Complexes with Tethered Pyridinyl and Propenyl Groups: Investigations of the Effect of Ring Size on Chelate Formation, Structure, and Linkage Isomerization
Authors of publication
Duke, Charles B.; Letterman, Roger G.; Johnson, Jermaine O.; Barr, James W.; Hu, Songnan; Ross, Charles R.; Webster, Charles Edwin; Burkey, Theodore J.
Journal of publication
Organometallics
Year of publication
2014
Journal volume
33
Journal issue
2
Pages of publication
485
a
11.2163 ± 0.0005 Å
b
9.8121 ± 0.0004 Å
c
12.7619 ± 0.0005 Å
α
90°
β
90.176 ± 0.002°
γ
90°
Cell volume
1404.51 ± 0.1 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0344
Residual factor for significantly intense reflections
0.0326
Weighted residual factors for significantly intense reflections
0.0861
Weighted residual factors for all reflections included in the refinement
0.0876
Goodness-of-fit parameter for all reflections included in the refinement
