Information card for entry 4082349

Structure parameters

• Formula: C65 H50 Cl2 N4 O12 Re4 Se4
• Calculated formula: C65 H50 Cl2 N4 O12 Re4 Se4
• Title of publication: Self-Assembly of Selenium-Bridged Rhenium(I)-Based Metalla Rectangles: Synthesis, Characterization, and Molecular Recognition Studies
• Authors of publication: Manimaran, Bala.; Vanitha, A.; Karthikeyan, M.; Ramakrishna, Buthanapalli; Mobin, Shaikh M.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 2
• Pages of publication: 465
• a: 11.1407 ± 0.0003 Å
• b: 13.8641 ± 0.0003 Å
• c: 23.4548 ± 0.0005 Å
• α: 92.962 ± 0.002°
• β: 102.495 ± 0.002°
• γ: 108.16 ± 0.002°
• Cell volume: 3332.94 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.134
• Residual factor for significantly intense reflections: 0.0632
• Weighted residual factors for significantly intense reflections: 0.0923
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 0.93
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No