Information card for entry 4082760

Structure parameters

• Formula: C149.17 H134 O14 Zn4
• Calculated formula: C149.176 H134 O14 Zn4
• Title of publication: Conversion Between Doubly and Triply Carboxylate-Bridged Di(ethylzinc) Complexes and Formation of the (μ-Oxo)tetrazinc Carboxylate [Zn4O(Ar(Tol)CO2)6].
• Authors of publication: Minier, Mikael A.; Lippard, Stephen J.
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 6
• Pages of publication: 1462 - 1466
• a: 15.384 ± 0.002 Å
• b: 19.152 ± 0.003 Å
• c: 23.061 ± 0.003 Å
• α: 68.151 ± 0.002°
• β: 89.974 ± 0.002°
• γ: 82.9 ± 0.002°
• Cell volume: 6250.5 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1198
• Residual factor for significantly intense reflections: 0.0656
• Weighted residual factors for significantly intense reflections: 0.145
• Weighted residual factors for all reflections included in the refinement: 0.1713
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No