Information card for entry 4082939

Structure parameters

• Formula: C76 H124 Cl8 N8 S10 Sn6
• Calculated formula: C76 H124 Cl8 N8 S10 Sn6
• Title of publication: Diamondoid Hydrazones and Hydrazides: Sterically Demanding Ligands for Sn/S Cluster Design
• Authors of publication: Barth, Beatrix E. K.; Tkachenko, Boryslav A.; Eußner, Jens P.; Schreiner, Peter R.; Dehnen, Stefanie
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 7
• Pages of publication: 1678
• a: 11.5634 ± 0.0009 Å
• b: 13.682 ± 0.0008 Å
• c: 16.8943 ± 0.0015 Å
• α: 77.9 ± 0.006°
• β: 70.783 ± 0.007°
• γ: 89.54 ± 0.006°
• Cell volume: 2462.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1473
• Residual factor for significantly intense reflections: 0.0545
• Weighted residual factors for significantly intense reflections: 0.0866
• Weighted residual factors for all reflections included in the refinement: 0.0954
• Goodness-of-fit parameter for all reflections included in the refinement: 0.806
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No