Nature Chooses Rings: Synthesis of Silicon-Containing Macrocyclic Peroxides
Authors of publication
Arzumanyan, Ashot V.; Novikov, Roman A.; Terent’ev, Alexander O.; Platonov, Maxim M.; Lakhtin, Valentin G.; Arkhipov, Dmitry E.; Korlyukov, Alexander A.; Chernyshev, Vladimir V.; Fitch, Andrew N.; Zdvizhkov, Alexander T.; Krylov, Igor B.; Tomilov, Yury V.; Nikishin, Gennady I.
Journal of publication
Organometallics
Year of publication
2014
Journal volume
33
Journal issue
9
Pages of publication
2230
a
9.9058 ± 0.0008 Å
b
11.5174 ± 0.001 Å
c
12.2235 ± 0.001 Å
α
99.111 ± 0.002°
β
113.255 ± 0.002°
γ
105.766 ± 0.002°
Cell volume
1176.11 ± 0.17 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0523
Residual factor for significantly intense reflections
0.042
Weighted residual factors for significantly intense reflections
0.1043
Weighted residual factors for all reflections included in the refinement
0.1092
Goodness-of-fit parameter for all reflections included in the refinement
