Information card for entry 4083183

Structure parameters

• Formula: C30 H32 Cl P Sn
• Calculated formula: C30 H32 Cl P Sn
• SMILES: [Sn]1(Cl)([P](c2ccc3c4c(ccc1c24)CC3)(C(C)C)C(C)C)(c1ccccc1)c1ccccc1
• Title of publication: Sterically Restricted Tin Phosphines, Stabilized by Weak Intramolecular Donor‒Acceptor Interactions
• Authors of publication: Athukorala Arachchige, Kasun S.; Sanz Camacho, Paula; Ray, Matthew J.; Chalmers, Brian A.; Knight, Fergus R.; Ashbrook, Sharon E.; Bühl, Michael; Kilian, Petr; Slawin, Alexandra M. Z.; Woollins, J. Derek
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 10
• Pages of publication: 2424
• a: 10.118 ± 0.005 Å
• b: 18.035 ± 0.008 Å
• c: 14.906 ± 0.007 Å
• α: 90°
• β: 93.905 ± 0.012°
• γ: 90°
• Cell volume: 2714 ± 2 ų
• Cell temperature: 125 K
• Ambient diffraction temperature: 125 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.0999
• Weighted residual factors for all reflections included in the refinement: 0.2758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.139
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No