Information card for entry 4084009

Structure parameters

• Formula: C31 H26 Cl O13 Os3 Sb
• Calculated formula: C31 H26 Cl O13 Os3 Sb
• SMILES: [Os]1([Os]([Sb]([Os]1(C#[O])(C#[O])(C#[O])C#[O])(c1ccccc1)c1ccccc1)(C#[O])(C#[O])(C#[O])Cl)(C#[O])(C#[O])(C#[O])C#[O].O1CCCC1.O1CCCC1
• Title of publication: Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings
• Authors of publication: Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3867
• a: 17.2925 ± 0.0003 Å
• b: 18.7276 ± 0.0003 Å
• c: 22.4687 ± 0.0003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7276.4 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0254
• Residual factor for significantly intense reflections: 0.0211
• Weighted residual factors for significantly intense reflections: 0.0433
• Weighted residual factors for all reflections included in the refinement: 0.0446
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No