Information card for entry 4084017

Structure parameters

• Formula: C38.7 H29.4 Cl3.4 O10 Os3 Sb2
• Calculated formula: C38.7 H29.4 Cl3.4 O10 Os3 Sb2
• Title of publication: Binuclear Oxidative Addition of Sb‒Cl Bonds: A Facile Synthetic Route to Main Group‒Transition Element Clusters and Rings
• Authors of publication: Li, Ying-Zhou; Ganguly, Rakesh; Leong, Weng Kee
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 14
• Pages of publication: 3867
• a: 12.7426 ± 0.0004 Å
• b: 14.632 ± 0.0004 Å
• c: 15.3921 ± 0.0005 Å
• α: 101.734 ± 0.0017°
• β: 105.35 ± 0.0017°
• γ: 108.723 ± 0.0017°
• Cell volume: 2486.98 ± 0.14 ų
• Cell temperature: 103 ± 2 K
• Ambient diffraction temperature: 103 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.0975
• Weighted residual factors for all reflections included in the refinement: 0.1078
• Goodness-of-fit parameter for all reflections included in the refinement: 1.187
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No