Information card for entry 4084113

Structure parameters

• Chemical name: [Pd2Cl2(Me)2(1,3-trans-dppcbO2)]
• Formula: C121.7 H116 Cl17.7 O4 P8 Pd4
• Calculated formula: C121.7 H116 Cl17.7 O4 P8 Pd4
• Title of publication: Linear α-Olefins Obtained with Palladium(II) Complexes Bearing a Partially Oxidized Tetraphosphane
• Authors of publication: Oberhauser, Werner; Manca, Gabriele; Ienco, Andrea; Strabler, Christof; Prock, Johannes; Weninger, Alexander; Gutmann, Rene; Brüggeller, Peter
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 15
• Pages of publication: 4067
• a: 15.5968 ± 0.0003 Å
• b: 17.3262 ± 0.0005 Å
• c: 26.5022 ± 0.0006 Å
• α: 108.414 ± 0.001°
• β: 105.187 ± 0.001°
• γ: 91.546 ± 0.001°
• Cell volume: 6510.5 ± 0.3 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0631
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for significantly intense reflections: 0.1259
• Weighted residual factors for all reflections included in the refinement: 0.1626
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No