Information card for entry 4084749

Structure parameters

• Formula: C102 H86 B Cl4 O Os P4
• Calculated formula: C102 H86 B Cl4 O Os P4
• Title of publication: Synthesis, Structure, and Reactivity of an Osmacyclopentene Complex
• Authors of publication: Han, Feifei; Wang, Tongdao; Li, Jinhua; Zhang, Hong; Zhang, Laiying; He, Xumin; Xia, Haiping
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5301
• a: 11.9935 ± 0.0003 Å
• b: 37.6087 ± 0.0007 Å
• c: 19.3005 ± 0.0008 Å
• α: 90°
• β: 101.956 ± 0.004°
• γ: 90°
• Cell volume: 8516.8 ± 0.5 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0923
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1203
• Weighted residual factors for all reflections included in the refinement: 0.1518
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No