Information card for entry 4084751

Structure parameters

• Formula: C61.5 H48 Cl N2 Os P3 S2
• Calculated formula: C61.5 H48 Cl N2 Os P3 S2
• Title of publication: Synthesis, Structure, and Reactivity of an Osmacyclopentene Complex
• Authors of publication: Han, Feifei; Wang, Tongdao; Li, Jinhua; Zhang, Hong; Zhang, Laiying; He, Xumin; Xia, Haiping
• Journal of publication: Organometallics
• Year of publication: 2014
• Journal volume: 33
• Journal issue: 19
• Pages of publication: 5301
• a: 12.6974 ± 0.0003 Å
• b: 21.4782 ± 0.0005 Å
• c: 19.9049 ± 0.0005 Å
• α: 90°
• β: 97.199 ± 0.002°
• γ: 90°
• Cell volume: 5385.6 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0422
• Residual factor for significantly intense reflections: 0.0309
• Weighted residual factors for significantly intense reflections: 0.0928
• Weighted residual factors for all reflections included in the refinement: 0.0952
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No