Information card for entry 4085234

Structure parameters

• Formula: C15 H23 Cl Fe Ge N2 O4
• Calculated formula: C15 H23 Cl Fe Ge N2 O4
• SMILES: C(#[O])[Fe](C#[O])(C#[O])(C#[O])[Ge]1([N](=C(C(C)(C)C)N1C(C)C)C(C)C)Cl
• Title of publication: Iron Complexes with Stabilized Germylenes: Syntheses and Characterizations
• Authors of publication: El Ezzi, Mohammad; Kocsor, Tibor-Gabor; D’Accriscio, Florian; Madec, David; Mallet-Ladeira, Sonia; Castel, Annie
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 571
• a: 11.4952 ± 0.0003 Å
• b: 13.611 ± 0.0004 Å
• c: 26.4708 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4141.7 ± 0.2 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0577
• Residual factor for significantly intense reflections: 0.0322
• Weighted residual factors for significantly intense reflections: 0.0839
• Weighted residual factors for all reflections included in the refinement: 0.0935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No