Information card for entry 4085251

Structure parameters

• Formula: C36 H96 I2 La2 N4 Si8
• Calculated formula: C36 H96 I2 La2 N4 Si8
• Title of publication: Homoleptic Trigonal Planar Lanthanide Complexes Stabilized by Superbulky Silylamide Ligands
• Authors of publication: Goodwin, Conrad A. P.; Joslin, Kristian C.; Lockyer, Selena J.; Formanuik, Alasdair; Morris, Gareth A.; Ortu, Fabrizio; Vitorica-Yrezabal, Iñigo. J.; Mills, David P.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2314
• a: 9.1458 ± 0.0006 Å
• b: 14.996 ± 0.0009 Å
• c: 22.8837 ± 0.0015 Å
• α: 94.293 ± 0.005°
• β: 96.373 ± 0.005°
• γ: 99.075 ± 0.005°
• Cell volume: 3066.4 ± 0.3 ų
• Cell temperature: 150.01 ± 0.16 K
• Ambient diffraction temperature: 150.01 ± 0.16 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1308
• Residual factor for significantly intense reflections: 0.0591
• Weighted residual factors for significantly intense reflections: 0.1005
• Weighted residual factors for all reflections included in the refinement: 0.1343
• Goodness-of-fit parameter for all reflections included in the refinement: 0.839
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No