Information card for entry 4085325

Structure parameters

• Formula: C46.88 H73 Cl0.75 F3 N2 O3.63 Os P S
• Calculated formula: C46.875 H73 Cl0.75 F3 N2 O3.625 Os P S
• Title of publication: Hydroboration and Hydrogenation of an Osmium‒Carbon Triple Bond: Osmium Chemistry of a Bis-σ-Borane
• Authors of publication: Buil, Mar\?ía L.; Cardo, Juan J. F.; Esteruelas, Miguel A.; Fernández, Israel; Oñate, Enrique
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 3
• Pages of publication: 547
• a: 12.112 ± 0.002 Å
• b: 12.152 ± 0.002 Å
• c: 35.128 ± 0.007 Å
• α: 81.728 ± 0.003°
• β: 86.522 ± 0.003°
• γ: 74.427 ± 0.003°
• Cell volume: 4927.4 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.0424
• Weighted residual factors for significantly intense reflections: 0.0978
• Weighted residual factors for all reflections included in the refinement: 0.1066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No