Information card for entry 4085428

Structure parameters

• Formula: C111 H172 Li4 N8 Si4
• Calculated formula: C111 H172 Li4 N8 Si4
• Title of publication: Group 1 Complexes of an (Amido-amino)silane and Their Use in the Synthesis of the Bi(III) Amide, Bi(Me2Si{NAr}{N(H)Ar})Cl2(Ar = 2,6-i-Pr2C6H3)
• Authors of publication: Schwamm, Ryan J.; Coles, Martyn P.; Fitchett, Christopher M.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 11
• Pages of publication: 2500
• a: 12.2412 ± 0.0003 Å
• b: 13.074 ± 0.0003 Å
• c: 20.0829 ± 0.0005 Å
• α: 105.704 ± 0.001°
• β: 93.758 ± 0.001°
• γ: 116.307 ± 0.001°
• Cell volume: 2708.84 ± 0.12 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0979
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.1404
• Weighted residual factors for all reflections included in the refinement: 0.1585
• Goodness-of-fit parameter for all reflections included in the refinement: 0.98
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No