Information card for entry 4086145

Structure parameters

• Formula: C48 H80 Ge P2 Ru
• Calculated formula: C48 H80 Ge P2 Ru
• Title of publication: A Ruthenium Dihydrogen Germylene Complex and the Catalytic Synthesis of Digermoxane
• Authors of publication: Smart, Katharine A.; Mothes-Martin, Emmanuelle; Vendier, Laure; Perutz, Robin N.; Grellier, Mary; Sabo-Etienne, Sylviane
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 16
• Pages of publication: 4158
• a: 9.9875 ± 0.0006 Å
• b: 12.5461 ± 0.0007 Å
• c: 19.5939 ± 0.0011 Å
• α: 80.397 ± 0.002°
• β: 88.455 ± 0.002°
• γ: 70.432 ± 0.002°
• Cell volume: 2279.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0253
• Residual factor for significantly intense reflections: 0.0232
• Weighted residual factors for significantly intense reflections: 0.0583
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No