Information card for entry 4086157

Structure parameters

• Formula: C94 H115 Ge2 N2 Si2
• Calculated formula: C94 H115 Ge2 N2 Si2
• Title of publication: Reactivity of Amido-Digermynes, LGeGeL (L = Bulky Amide), toward Olefins and Related Molecules: Facile Reduction, C–H Activation, and Reversible Cycloaddition of Unsaturated Substrates
• Authors of publication: Hadlington, Terrance J.; Li, Jiaye; Hermann, Markus; Davey, Amelia; Frenking, Gernot; Jones, Cameron
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 13
• Pages of publication: 3175
• a: 12.147 ± 0.002 Å
• b: 18.15 ± 0.004 Å
• c: 21.586 ± 0.004 Å
• α: 66.86 ± 0.03°
• β: 74.62 ± 0.03°
• γ: 74.2 ± 0.03°
• Cell volume: 4142.9 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0472
• Residual factor for significantly intense reflections: 0.0416
• Weighted residual factors for significantly intense reflections: 0.1048
• Weighted residual factors for all reflections included in the refinement: 0.108
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.7108 Å
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No