Information card for entry 4086180

Structure parameters

• Formula: C34 H48 B11 Cl11 P2 Pt Si
• Calculated formula: C34 H48 B11 Cl11 P2 Pt Si
• Title of publication: Silyl‒Silylene Interplay in Cationic PSiP Pincer Complexes of Platinum
• Authors of publication: DeMott, Jessica C.; Gu, Weixing; McCulloch, Billy J.; Herbert, David E.; Goshert, Mitchell D.; Walensky, Justin R.; Zhou, Jia; Ozerov, Oleg V.
• Journal of publication: Organometallics
• Year of publication: 2015
• Journal volume: 34
• Journal issue: 16
• Pages of publication: 3930
• a: 8.8067 ± 0.001 Å
• b: 16.4732 ± 0.0019 Å
• c: 18.252 ± 0.002 Å
• α: 93.859 ± 0.001°
• β: 93.163 ± 0.001°
• γ: 95.343 ± 0.001°
• Cell volume: 2625.4 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0455
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.0935
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No