Crystallography Open Database

Information card for entry 4086347

Preview

Coordinates	4086347.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	PNP(iPr)Dy(H)2Ru(C5Me5)PPh2(CH2)
Formula	C52 H76 Dy N P3 Ru
Calculated formula	C52 H76 Dy N P3 Ru
Title of publication	PNP-Ligated Heterometallic Rare-Earth/Ruthenium Hydride Complexes Bearing Phosphinophenyl and Phosphinomethyl Bridging Ligands
Authors of publication	O, Wylie W. N.; Kang, Xiaohui; Luo, Yi; Hou, Zhaomin
Journal of publication	Organometallics
Year of publication	2014
Journal volume	33
Journal issue	4
Pages of publication	1030 - 1043
a	12.5336 ± 0.0008 Å
b	13.2381 ± 0.0008 Å
c	18.2036 ± 0.0012 Å
α	99.641 ± 0.003°
β	102.993 ± 0.002°
γ	113.592 ± 0.002°
Cell volume	2582.5 ± 0.3 Å³
Cell temperature	163 ± 2 K
Ambient diffraction temperature	163 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0514
Residual factor for significantly intense reflections	0.0378
Weighted residual factors for significantly intense reflections	0.0862
Weighted residual factors for all reflections included in the refinement	0.0914
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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