Crystallography Open Database

Information card for entry 4086722

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Coordinates	4086722.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H30 Mg O2
Calculated formula	C22 H30 Mg O2
Title of publication	Mechanism of Alkyl Migration in Diorganomagnesium 2,6-Bis(imino)pyridine Complexes: Formation of Grignard-Type Complexes with Square-Planar Mg(II) Centers
Authors of publication	Sandoval, John J.; Palma, Pilar; Álvarez, Eleuterio; Cámpora, Juan; Rodríguez-Delgado, Antonio
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	18
Pages of publication	3197
a	9.37 ± 0.0007 Å
b	9.0598 ± 0.0006 Å
c	12.5313 ± 0.0008 Å
α	90°
β	100.684 ± 0.002°
γ	90°
Cell volume	1045.34 ± 0.12 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0814
Residual factor for significantly intense reflections	0.0624
Weighted residual factors for significantly intense reflections	0.1747
Weighted residual factors for all reflections included in the refinement	0.2081
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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