Information card for entry 4086839

Structure parameters

• Common name: (PNP-tBu)YNp2
• Formula: C32 H64 N P2 Y
• Calculated formula: C32 H64 N P2 Y
• SMILES: C(C(C)(C)C)[Y]12(CC(C)(C)C)n3c(C[P]1(C(C)(C)C)C(C)(C)C)ccc3C[P]2(C(C)(C)C)C(C)(C)C
• Title of publication: Evidence for the Existence of Group 3 Terminal Methylidene Complexes
• Authors of publication: Levine, Daniel S.; Tilley, T. Don; Andersen, Richard A.
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 1
• Pages of publication: 80
• a: 11.2268 ± 0.0004 Å
• b: 18.2514 ± 0.0007 Å
• c: 18.4495 ± 0.0007 Å
• α: 95.262 ± 0.002°
• β: 107.167 ± 0.002°
• γ: 96.588 ± 0.002°
• Cell volume: 3556.6 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0744
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.0719
• Weighted residual factors for all reflections included in the refinement: 0.0804
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No