Zirconocene-Based Methods for the Preparation of BN-Indenes: Application to the Synthesis of 1,5-Dibora-4a,8a-diaza-1,2,3,5,6,7-hexaaryl-4,8-dimethyl-s-indacenes
Authors of publication
Morgan, Matthew M.; Patrick, Evan A.; Rautiainen, J. Mikko; Tuononen, Heikki M.; Piers, Warren E.; Spasyuk, Denis M.
Journal of publication
Organometallics
Year of publication
2017
a
7.5793 ± 0.0005 Å
b
20.7341 ± 0.0011 Å
c
12.3247 ± 0.0005 Å
α
90°
β
94.596 ± 0.004°
γ
90°
Cell volume
1930.6 ± 0.18 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0671
Residual factor for significantly intense reflections
0.0478
Weighted residual factors for significantly intense reflections
0.1164
Weighted residual factors for all reflections included in the refinement
0.1269
Goodness-of-fit parameter for all reflections included in the refinement
