Zirconocene-Based Methods for the Preparation of BN-Indenes: Application to the Synthesis of 1,5-Dibora-4a,8a-diaza-1,2,3,5,6,7-hexaaryl-4,8-dimethyl-s-indacenes
Authors of publication
Morgan, Matthew M.; Patrick, Evan A.; Rautiainen, J. Mikko; Tuononen, Heikki M.; Piers, Warren E.; Spasyuk, Denis M.
Journal of publication
Organometallics
Year of publication
2017
a
19.31 ± 0.02 Å
b
17.619 ± 0.014 Å
c
24.71 ± 0.02 Å
α
90°
β
90°
γ
90°
Cell volume
8407 ± 13 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
6
Space group number
61
Hermann-Mauguin space group symbol
P b c a
Hall space group symbol
-P 2ac 2ab
Residual factor for all reflections
0.0786
Residual factor for significantly intense reflections
0.0612
Weighted residual factors for significantly intense reflections
0.1614
Weighted residual factors for all reflections included in the refinement
0.1776
Goodness-of-fit parameter for all reflections included in the refinement
